@Wes Christensen No I didn’t try that I thought I couldn’t add anymore since I already add 3ml for that blend

Yes it’s a brand new vial and happened right the next day when I check. “They just answer my email saying this The particles shown in your photos look more consistent with undissolved peptide material, crystallization, or aggregation of ingredients, rather than any indication of biological contamination. Some commonly noted contributing factors include diluent being injected directly onto the powder cake with too much force, insufficient time allowed for full hydration, repeated warming and cooling cycles, or storage at colder temperatures shortly after mixing.” So I think I’m good to go on that one